By S. Velumani and René Asomoza
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Extra info for Advances in Semiconducting Materials
4 shows the XRD patterns and the SEM images of several sample surfaces. Fig. 4 (a) shows the results for the as-sintered specimen in which only Ni and α-Al2O3 peaks were detected and no other crystalline phases were observed. Fig. 4 (b) shows the sample annealed at 1300°C for 3 h. The cracks were completely disappeared. As shown in the SEM image; fine and well-faceted particles are observed on the whole surface. As XRD analysis shows, this product consists of NiAl2O4 spinel. When the same conditions (1300°C for 3 h) were used under an Ar+1%H2 gas mixture, significant changes in the crack are observed, as shown in Fig.
3357-3361.  M. Cooper, and K. 614-617. F. Mondolfo, Aluminum Alloys, Structures and Properties, 1st. Ed. , London 1976, pp. 661-663.  M. , Vol. 23. 1967, pp. 1106-1107.  A. Toscano, PhD. Thesis, “Processing and Microstructure of AlFeMnSi Intermetallic Compounds By High Temperature Reactive Sintering”. CINVESTAV-IPN, Unidad Saltillo, México, March 2002.  R. al, J. Phys. & Condens. Matter, 1990, 2, p. 3855.  FULLPROF. 5 (PC-version), December 1997. A. B. Brook, Editors, Smithells Metals Reference Book, 7th Edition.
Sato. Crack-healing and oxidation behavior of silicon nitride ceramics. 2329–2338.  K. Ando, K. Furusawa, K. Takahashi, S. Sato. Crack-healing ability of structural ceramics and a new methodology to guarantee the structural integrity using the ability and proof-test. Journal of the European Ceramic Society, 25 (2005) pp. 549-558.  C. Zdenek, F. Petr, K. Ando, D. Ivo. Fracture Behaviour of Al2O3/SiC nanocomposite ceramics after crack healing treatment. Journal of the European Ceramic Society, 28 (2008) pp.
Advances in Semiconducting Materials by S. Velumani and René Asomoza